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By International Atomic Energy Agency

ISBN-10: 9201147031

ISBN-13: 9789201147035

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Why nuclear analytical techniques? The X ray fluorescence (XRF) technique in the energy dispersive mode (EDXRF) has been used to deal with these analytical problems. XRF spectrometry is a well established instrumental analytical technique used for chemical composition analysis. XRF is a non-destructive multielement technique capable of determining elements with atomic number Z ≥ 11 (sodium) in different matrices. The samples to be analysed require minimal or no preparation, and the technique is regarded as non-destructive.

Mater. 83 (2001) 93–122. Report of the First Research Coordination Mtg under the Coordinated Research Project on In Situ Applications of XRF Techniques, IAEA, Vienna, 2001. A. (Eds), Handbook of X-Ray Spectrometry, Dekker, New York (2002). Part II 40 Advanced X ray fluorescence techniques Si(Li) detector CCD camera and microscope SDD detector Sample Motorized scanning stage Focusing glass capillary X ray tube FIG. 1. Schematic view of the microbeam XRF system. FIG. 2. Uranium rich and iron rich particles.

The radioindicator had been produced through a photonuclear reaction by irradiating U3O8 containing natural uranium with the bremsstrahlung of an electron linear accelerator. Over a total experimental period of about 800 h the uranium migration front was monitored by regularly scheduled scanning measurement of the photon emission of the radioindicator along the length of the column. This experiment was repeated using different concentrations of sorbents. The results allowed the time of breakthrough of the uranium at the end of the sorbent layer to be predicted with high precision.

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Analytical applications of nuclear techniques by International Atomic Energy Agency

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