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By J. S. Fruchter, C. L. Wilkerson, J. C. Evans, R. W. Sanders (auth.), Royston H. Filby, B. Stephen Carpenter, Richard C. Ragaini (eds.)

ISBN-10: 1468441337

ISBN-13: 9781468441338

ISBN-10: 1468441353

ISBN-13: 9781468441352

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Eng. Data. 5:5533 (1967) ~. 4. A. Skinner, Ind. Chern. Eng. 44:1159 (1952) 5. H. E. S. G. L. , Amer. Chern. - G. P. H. - 7. A. Treibs, Ann. :42 (1934) 8. G. Bertrand, R. Paulais, Cornp. - 9. E. A. Gleborskaya, M. V. ) 18:440. (1948) ~ Gen. , W. B. Shirey, Ind. 11. G. W. Hodgson, Bull. Amer. Assoc, Petrol. Geol. 38;2531 (1954). -- -- --- 12. J. Hyden, 13. H. J. Al-Atiya, Geochirn. et Cosrnochirn. - 14. Y. N. P. Kurstalskaya, Tr. Vses. Neft. Nank. Issled. Geol. =- 15. F. G. N. Berturina, Tr. Tater.

Minerals and trace metals present as different types of molecules. Upgrading of crudes is to a great extent the elimination, by physical or chemical methods, of these non-hydrocarbon components as well as the removal of the high molecular weight fraction called asphaltenes. As a general rule, trace metal content in crude oil increases with its asphaltene yield. It is a well known fact that as the crude becomes lighter (higher API £), its metal content becomes lower. The API gravity increases as the oil becomes more mature.

A. 5 to 1500 ppb. Due to the very low concentration of Cadmium in crudes, it cannot be determined instrumentally. A novel radiochemical separation has been developed at INTEVEP to determine cadmium at sub-ppm levels which has proven to be quantitive and precise. Samples and standards were submitted to irradiation for 40 hr. cm L • sec -1. After irradiation, each sample was quantitatively transfered to a Bethge digestion apparatus and cadmium carrier was added. Mineralization was performed using a mixture of H2S04 HN0 3 - HCl0 4 • The final solution is extracted with n-hexane and partially neutralized to pH of 6.

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Atomic and Nuclear Methods in Fossil Energy Research by J. S. Fruchter, C. L. Wilkerson, J. C. Evans, R. W. Sanders (auth.), Royston H. Filby, B. Stephen Carpenter, Richard C. Ragaini (eds.)


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